https://doi.org/10.15255/KUI.2016.025
Published: Kem. Ind. 66 (7-8) (2017) 345−351
Paper reference number: KUI-25/2016
Paper type: Original scientific paper
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Effect of Solid Solution and Ageing Treatments on the Microstructure and Mechanical Properties of the SiCp/Al-Si-Cu-Mg Composite

A. Q. Wang, H. D. Guo, H. H. Han and J. P. Xie

Abstract

The SiC particles (SiCp, mass fraction 30 %) reinforced with the Al-Si-Cu-Mg matrix composite have been prepared using one-way press method, sintering, and hot extrusion. The composite was subjected to solid solution treatment at temperatures of 470 °C, 485 °C, 500 °C, 515 °C, and 530 °C for 4 h. The sample was then subjected to ageing treatment at temperatures of 160 °C and 180 °C during different times after solid solution treatment at 515 °C for 4 h. The microstructure and mechanical properties of the SiCp/Al-Si-Cu-Mg matrix composite under the different ageing and solid solution treatments were tested using SEM and TEM microhardness analysis. The results show that the white granulated metallic compounds of the SiCp/Al-Si-Cu-Mg composite materials, which are formed in the sintering process of composite materials, dissolve back after the solid solution treatment at different temperatures. The higher the solid solution temperature, the more metallic compounds dissolve back. The microhardness of the composites reached maximum after solution treatment at 515 °C for 4 h. Following the ageing treatment and with the prolongation of ageing time, the hardness of the composite material reached “double peak” phenomenon. With the increase in ageing temperature, the hardening speed of the composite material also increased, but at the same time, the hardening ability had reduced. After the ageing treatment, the second phases of the composite are discoid Al₅Cu₆Mg₂.

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Keywords

SiCp/Al-Si-Cu-Mg composite, solid solution treatment, ageing treatment, microstructure, microhardness